直接灰吹法测定金泥中金和银的研究

通过对铅捕集贵金属原理的研究,首次提出铅覆盖再次富集的概念,建立了高品位金泥中金、银的检测方法。以经典火试金法测得的金银含量为准确值,计算金泥直接灰吹对金银的回收率,探讨了铅箔用量、称样量、灰吹温度和铅箔覆盖方式对金银回收率的影响,获得了高品位金泥直接灰吹的最佳工艺条件。在最佳工艺条件下,对氰化-置换得到的高品位金泥进行直接灰吹法与火试金方法对比试验,结果显示直接灰吹法的分析结果与火试金重量法结果相吻合。 金的回收率为99.84-100.12%,RSD≤0.10%(n=6),银的回收率为99.41-100.66,RSD≤0.40%(n=6)。该方法操作简便、快捷准确,劳动强度低,有很好的适用性。     

Feasibility and extension of universal quantitative models for moisture content determination in beta-lactam powder injections by near-infrared spectroscopy

In present work, we investigated the feasibility of universal calibration models for moisture content determination of a much complicated products system of powder injections to simulate the process of building universal models for drug preparations with same INN (International Nonproprietary Name) from diverse formulations and sources. We also extended the applicability of universal model by model updating and calibration transfer. Firstly, a moisture content quantitative model for ceftriaxone sodium for injection was developed, the results show that calibration model established for products of some manufacturers is also available for the products of others. Then, we further constructed a multiplex calibration model for seven cephalosporins for injection ranging from 0.40 to 9.90%, yielding RMSECV and RMSEP of 0.283 and 0.261, respectively. However, this multiplex model could not predict samples of another cephalosporin (ceftezole sodium) and one penicillins (penicillin G procaine) for injection accurately. With regard to such limits and the extension of universal models, two solutions are proposed: model updating (MU) and calibration transfer. Overall, model updating is a robust method for the analytical problem under consideration. When timely model updating is impractical, piecewise direct standardization (PDS) algorithm is more desirable and applied to transfer calibration model between different powder injections. Both two solutions have proven to be effective to extend the applicability of original universal models for the new products emerging.     

Fractional Fourier transform on R2 and an application

We focus on the L^p(R²) theory of the fractional Fourier transform (FRFT) for 1 ≤ p ≤ 2. In L¹(R²), we mainly study the properties of the FRFT via introducing the two-parameter chirp operator. In order to get the point-wise convergence for the inverse FRFT, we introduce the fractional convolution and establish the corresponding approximate identities. Then the well-defined inverse FRFT is given via approximation by suitable means, such as fractional Gauss means and Able means. Furthermore, if the signal F_α,βf is received, we give the process of recovering the original signal f with MATLAB. In L²(R²), the general Plancherel theorem, direct sum decomposition, and the general Heisenberg inequality for the FRFT are obtained.     

关于模糊拓扑环的直积

给出模糊拓扑环族直积的定义,研究它的性质,及任意模糊拓扑环族直积、与其模糊拓扑子环,与其模糊拓扑剩余环之间的同构问题.并对(QU)型模糊拓扑环关于上述问题进行研究.     

激光二极管列阵侧面直接抽运方式的模拟计算和效果评估

计算模拟了激光二极管侧面直接抽运方式，讨论了抽运距离和介质吸收系数等参数对抽运均匀性的影响，并近似地给出定量结果，证明只要选取适当的抽运参数，采用侧面直接抽运方式也能获得较好的抽运性能和激光输出。     

域上的线性变换

本文主要获得了任意域上的可逆线性变换群形如（1．1）的分解，是对有限域上的结果的推广。     

几类Lurie型控制系统绝对稳定性充分必要条件

本借助部分变元绝对稳定性的充要条件，得出几类Lurie型控制系统绝对稳定性充分必要条件，这些判据为显式的代数形式，易于验证，也便于在实践中应用。     

双面金属包覆介质波导的直接耦合方法

根据双面金属包覆介质波导的特殊性质，提出了一种新的波导耦合方法，这种技术在不用棱镜、光栅和其它元件的情况下，可使光能从金属表面直接耦合进波导。实验结果与理论预言符合得很好。     

Separability,gauge invariance and nonsuperluminality in direct interaction dynamics

We discuss the classical mechanics of relativistic systems with direct interaction. We show that various desiderata can all be accommodated in the single time approach by restricting the observables to the gauge invariant variables. We show how such observables can be constructed in general. We explicitly construct position observables in a general system and show that they lead to separable, invariant world lines. Nonsuperluminality is explicitly demonstrated for two body systems interacting via central forces of semibounded magnitude provided they ensure timelike canonical momenta. For two particles, our results reproduce the usual solution in covariant equal-time gauge.     

Determination of Boron with Isotope Dilution Method

100 ng or less amount of boron in the form of Na₂B₄O₇ was loaded on tantalum filament of thermal ionization mass spectrometer. A serial isotope ratios of metaborate, Me=88 (Na₂ ¹¹BO₂) and Me=89 (Na₂ ¹¹BO₂) prepared with spike (¹⁰B enriched) and nature boron were determined successfully and compared with reference values.